알림
뒤로

Bulk electrolysis

Category

Bulk electrolysis basic cell kit

Features


• 기본 bulk electrolysis cell kit

• 용액의 용량 대비 큰 표면적의 그물모양 Glassy carbon electrode 적용

• Gas-tight

Product Type


Product typeCat. No.
Aqueous
C-A-BULK_E_BC-50
Organic
C-O-BULK_E_BC-50

Specifications


Max. electrolyte volume
50 ml
Pt wire CE
Dia.0.6 mm, length 250 mm
Reticulated glassy carbonBulk density0.05 g/cm³
Porosity96.5 %
Resistivity400 μΩ•cm
Number of pores24 pores / cm
(60 pores / inch)
Wire contactTantalum wire, dia. 0.6 mm, length 60 mm
Cell materials
Glass, PEEK
O-Ring materials

FKM / EPDM (Aqueous)

FFKM (Organic)

Electrode plug diameter
6 mm

Components


• 50 ml glass cell x 1

• Lid x 1

• Pt CE x 1

• Ag/AgCl RE x 1 (or non-aqueous Ag/Ag+ RE x 1)

• Reticulated Glassy (Vitreous) carbon electrode x 1

• Plug x 1

Bulk electrolysis two-compartment cell kit

Features


• Two-compartment bulk electrolysis cell kit

• CE 는 WE 및 RE 와는 별도로 Ceramic frit 으로 분리된 glass cell 에 장착

• 용액의 용량 대비 큰 표면적의 그물모양 Glassy carbon electrode

• Gas-tight

Product Type


Product typeCat. No.
Aqueous
C-A-BULK_E_2C-50
Organic
C-O-BULK_E_2C-50

Specifications


Max. electrolyte volume
50 ml
Volume of CE compartment1.5 ml
Pt wire CE
Dia. 0.6 mm, length 250 mm
Reticulated glassy carbonBulk density0.05 g/cm³
Porosity96.5 %
Resistivity400 μΩ•cm
Number of pores24 pores / cm
(60 pores / inch)
Wire contactPlatinum wire, dia. 0.6 mm, length 60 mm
Cell materials
Glass, PEEK
O-Ring materials

FKM / EPDM (Aqueous)

FFKM (Organic)

Electrode plug diameter
6 mm

Components


• 50 ml glass cell x 1

• Lid x 1

• Pt CE x 1

• CE glass compartment x 1

• Ag/AgCl RE x 1 (or non-aqueous Ag/Ag+ RE x 1)

• Reticulated Glassy (Vitreous) carbon electrode x 1

• Plug x 1

Bulk electrolysis GC cell kit

Features


• Single compartment bulk electrolysis cell 로, 보통의 glass cell 이 아닌 glassy carbon 으로 만들어져 cell 이면서 동시에 WE 으로 작용

• Copper contact 가 cell 과 lid 사이에 ring 형태로 장착되며, 바닥의 PTFE insulation cup 을 통해 절연되어 있음. 

• 응용

  • Complete oxidation or reduction of species
  • Complete synthesis of a product through electrochemical processes
  • Partial oxidation or reduction of a compound
  • Studying the complexity of the reaction mechanism

• Liquid-/Gas-tight

Components


• Glassy carbon chamber x 1

• Lid x 1

• Pt CE x 1

• Ag/AgCl RE x 1 (or non-aqueous Ag/Ag+ RE x 1)

• Copper working electrode contact x 1

• Plug x 1 (or x 3 depends on option)

• Insulating PTFE cup x 1

• Set of fittings x 1

• Set of O-rings x 1

Product Type


Max. volumeAqueous
Organic
7 mlB-A-BULK_E_GC-7
B-O-BULK_E_GC-7
15 mlB-A-BULK_E_GC-15
B-O-BULK_E_GC-15
20 mlB-A-BULK_E_GC-20
B-O-BULK_E_GC-20
40 mlB-A-BULK_E_GC-40
B-O-BULK_E_GC-40
60 mlB-A-BULK_E_GC-60
B-O-BULK_E_GC-60
90 mlB-A-BULK_E_GC-90
B-O-BULK_E_GC-90
125 mlB-A-BULK_E_GC-125
B-O-BULK_E_GC-125
250 mlB-A-BULK_E_GC-250
B-O-BULK_E_GC-250
340 mlB-A-BULK_E_GC-340
B-O-BULK_E_GC-340
790 mlB-A-BULK_E_GC-790
B-O-BULK_E_GC-790

Specifications


Lid entry depth8.25 mm
Copper working electrode contactThickness 0.75 mm ring
Pt wire CE
Dia. 0.6 mm, length 250 mm
Glassy carbon chamberMax. temperature3,000 °C
(under vacuum or inert gas)
Density1.42 g/cm³ 
Open porosity0 %
Permeability coefficient10(-9)cm²/s
Vickers hardness230 HV
Specific electrical resistance at 30 °C45 Ωµm 
Thermal conductivity at 30 °C6.3 W/(Km)
Median linear coefficient of expansion (20-200°C )2.6 x 10(-6)1/K
Cell materials
PEEK, PTFE
O-Ring materials

FKM / EPDM (Aqueous)

FFKM (Organic)

Electrode plug diameter
6 mm

Glassy carbon chamber dimensions


Max. liquid volumeIDH (GC chamber depth)Wall thicknessNumber of ports
7 ml19 mm34 mm3 mm2 x 6 mm dia. port
15 ml24 mm42 mm3 mm2 x 6 mm dia. port
20 ml30 mm40 mm3 mm4 x 6 mm dia. port
40 ml35 mm51 mm3 mm4 x 6 mm dia. port
60 ml34 mm75 mm5 mm4 x 6 mm dia. port
90 ml43 mm73 mm3 mm4 x 6 mm dia. port
125 ml50 mm73 mm3 mm4 x 6 mm dia. port
250 ml68 mm79 mm3 mm4 x 6 mm dia. port
340 ml61 mm125 mm3 mm4 x 6 mm dia. port
790 ml98 mm113 mm3 mm4 x 6 mm dia. port